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针对木质化海芦笋因盐分含量高而难以直接还田或用作堆肥原料的问题,本研究对比了普通浸提、微波和超声波提取三种方法对海芦笋植物盐的提取效果差异,并确定最优提取工艺。结果表明:普通浸提的提取温度、提取时间和料液比均对海芦笋植物盐提取具有显著影响,在提取温度60℃、料液比1∶24(g/mL)、提取时间0.5 h条件下,海芦笋植物盐提取效果最佳;微波法最佳工艺为料液比1∶32(g/mL)、微波功率640W、提取时间10 min,其中料液比对海芦笋植物盐的提取影响显著,提取功率与提取时间存在交互作用;在料液比1∶24(g/mL)、时间5 min、温度40℃时的超声波提取效果最优,三因素对海芦笋植物盐提取量均无显著影响。在各自最佳条件下,三种方法所得的海芦笋精盐提取量无显著差异,但粗盐提取量因有机物溶出程度不同而差异显著。综合操作便捷性、时效性及粗盐提取量等因素,确定超声波法为提取海芦笋植物盐的最佳方法。
Abstract:High salt content in lignified Salicornia europaea prevents its direct recycling or composting on land. The extraction efficiency of plant salt from Salicornia europaea using maceration,microwave-assisted,and ultrasonicassisted methods were compared to determine the optimal extraction process. The results showed that,during maceration,extraction temperature,solid-to-liquid ratio,and extraction time all had significant effects on the extraction of plant salt,with the optimal conditions being an extraction temperature of 60 ℃,a solid-to-liquid ratio of 1∶24(g/mL),and an extraction time of 0.5 h. For microwave-assisted extraction,the solid-to-liquid ratio had the greatest effect,while power and time exhibited interactions;the optimal conditions were a solid-to-liquid ratio of 1∶32(g/mL),640 W,and 10 min. For ultrasonic-assisted extraction,the optimal conditions were a solidto-liquid ratio of 1∶24(g/mL),an extraction time of 5 min,and an extraction temperature of 40 ℃,under which none of the three factors showed a significant effect on the extraction yield. Refined salt yields were similar across all three methods;crude salt yields varied significantly due to the presence of organic matter. Considering operational convenience,time efficiency,and crude salt yield,ultrasonic-assisted extraction was identified as the optimal method.
[1]黄丹.多品种盐的开发研究[J].中国井矿盐,2004,35(3):39-42.
[2]王瑞华,孙佳佳,戴华磊,等.不同干燥方式对碱蓬植物盐品质特性的影响[J].食品研究与开发,2018,39(18):102-106.
[3]李煦,田鑫奥,倪睿杰,等.碱蓬植物盐提取工艺优化及其矿物质元素测定[J].食品安全质量检测学报,2022,13(22):7339-7347.
[4]张裕泽.海蓬子植物盐的制备及其化学成分的研究[D].天津:天津医科大学,2017.
[5]倪建伟.白刺植物盐提取技术与制备工艺研究[D].北京:中国林业科学研究院,2012.
[6]高叶颖,鞠云,刘光辉,等.海芦笋植物盐提取工艺的优化[J].中国食品添加剂,2020,31(8):60-66.
[7]Gunning D. Cultivating Salicornia europaea(marsh samphire)[J]. Dublin,Ireland:Irish Sea Fisheries Board, 2016, 4:1-95.
[8]Patel S. Salicornia:Evaluating the halophytic extremophile as a food and a pharmaceutical candidate[J]. 3 Biotech, 2016, 6:104.
[9]Ventura Y,Sagi M. Halophyte crop cultivation:The case for Salicornia and Sarcocornia[J]. Environmental and Experimental Botany,2013,92:144-153.
[10]王楠.海蓬子标准组分制备及其物质基础研究[D].青岛:中国海洋大学,2014.
[11]Cárdenas-Pérez S,Piernik A,Chanona-Pérez J J,et al. An overview of the emerging trends of the Salicornia L. genus as a sustainable crop[J]. Environmental and Experimental Botany,2021,191:104606.
[12]Ekanayake S,Egodawatta C,Attanayake R N,et al. From salt pan to saucepan:Salicornia,a halophytic vegetable with an array of potential health benefits[J]. Food Frontiers,2023,4(2):641-676.
[13]Mendis C L,Padmathilake R E,Attanayake R N,et al.Learning from Salicornia:Physiological,biochemical,and molecular mechanisms of salinity tolerance[J]. International Journal of Molecular Sciences,2025,26(13):5936.
[14]McNeely J D,Windham B G,Anderson D E. Dietary sodium effects on heart rate variability in salt sensitivity of blood pressure[J]. Psychophysiology,2008,45(3):405-411.
[15]Lee G H. A salt substitute with low sodium content from plant aqueous extracts[J]. Food Research International,2011,44(2):537-543.
[16]Wick C D,Dang L X,Jungwirth P. Simulated surface potentials at the vapor-water interface for the KCl aqueous electrolyte solution[J]. The Journal of Chemical Physics,2006,125(2):024706.
[17]Braschi A,Gill L,Naismith D J. Partial substitution of sodium with potassium in white bread:Feasibility and bioavailability[J]. International Journal of Food Sciences and Nutrition,2009,60(6):507-521.
[18]徐娜.韩国开发出具有保健功效的植物盐[J].福建农业,2008(9):39.
[19]任红星,吴世华,李建伟,等.一种海芦笋水溶性生物盐及其制备方法:CN101791108A[P]. 2010-08-04.
[20]刘凯文.海芦笋高钾低钠盐提取及速食汤料包的开发[D].天津:天津科技大学,2023.
[21]Kong C S,Kim J A,Qian Z J,et al. Protective effect of isorhamnetin 3-O-β-d-glucopyranoside from Salicornia herbacea against oxidation-induced cell damage[J]. Food and Chemical Toxicology,2009,47(8):1914-1920.
[22]Yuan Y F,Jin A M,Neal B,et al. Salt substitution and saltsupply restriction for lowering blood pressure in elderly care facilities:A cluster-randomized trial[J]. Nature Medicine,2023,29(4):973-981.
[23]陈宝印,郑清,邵荣,等.浅析植物盐的研究现状[J].安徽农学通报,2019,25(S1):109-112.
[24]刘素华,刘好鑫,尹金珠,等.响应面法优化盐地碱蓬中植物盐提取工艺的研究[J].食品工业,2017, 38(3):74-78.
[25]高叶颖.海芦笋植物盐的提取及低盐沙拉酱的开发研究[D].天津:天津科技大学,2022.
[26]袁连山,顾国亮,廖传华,等.微波对萃取过程的强化[J].香料香精化妆品,2005(1):29-32.
[27]纪耀华,马爱民,孙莹,等.大黄多糖传统水提法最佳工艺优化研究[J].时珍国医国药,2010,21(3):634-635.
[28]于永.微波在提取天然产物化学成分中的应用[D].长春:吉林大学,2008.
[29]薛宏坤,谭佳琪,蔡旭,等.微波功率对蔓越莓花色苷萃取过程的影响机理[J].食品科学,2022,43(1):92-101.
[30]王丽昀.微波辅助提取天然产物有效成分工艺研究[D].北京:北京化工大学,2010.
[31]余小影,易湘茜,高程海,等.碱蓬植物盐提取工艺研究[J].轻工科技,2018(8):1-4.
[32]李娜.超声辅助提取苦菜单宁的工艺优化及其动力学研究[D].西安:陕西师范大学,2012.
[33]刘星宇,廖艺超,王壹,等.超声波联用技术在植物活性成分提取中的应用研究进展[J].食品与发酵工业,2022,48(14):319-327.
[34]李婧怡,王玮棋,杨柳青,等.过氧化氢预处理-硝酸银滴定法测定氯离子的研究[J].中国土壤与肥料,2024(7):241-248.
基本信息:
DOI:10.19804/j.issn1006-2513.2026.5.004
中图分类号:TS36
引用信息:
[1]张宇婧,李婧怡,邱琦,等.浸提、微波和超声法的海芦笋植物盐提取效果差异研究[J].中国食品添加剂,2026,37(05):33-40.DOI:10.19804/j.issn1006-2513.2026.5.004.
基金信息:
中央引导地方科技发展资金(天津市优秀农业科技特派员项目)-盐生植物/甜土作物间作在盐碱地改良中的研究应用(24ZYCGSN1350); 大学生创新创业训练项目-碱蓬改良盐碱土壤及碱蓬的资源化利用(202410061092)
2026-05-15
2026-05-15
2026-05-15